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D1 Evolution

A comprehensive suite of superior X-ray metrology tools

Jordan Valley’s D1 Evolution is the latest generation of flexible X-ray diffraction instruments for thin-film materials research, process development, and quality control. Featuring fully automated source optics, the system can switch between standard XRD, High-Resolution, and X-ray reflectivity modes without user intervention. Measurements can be run in partial or fully automated modes, with user-customizable scripts handling the routine work. The instrument is designed for a variety of thin-film applications, including high resolution rocking curves, reciprocal space mapping, X-ray topography (digital imaging), X-ray reflectivity, Grazing Incidence XRD, Phase ID, residual stress, film texture and grain size analysis. The sample stage consists of a robust 5-axis Eulerian cradle, with 150 mm wafer mapping, and capacity for both large and small samples, and multi-sample locations. Leading edge data analysis packages, such as RADS and REFS provide expert data presentation and interpretation. The D1 Evolution is the ideal, multi-application thin-film materials research tool – for now and into the future.

The D1 is a materials research and development system for 200mm processes and below. Intended for use with Silicon, III/V, SiC, LED, Solar, Research and Development, & Universities.

Tool brochures can be found here.

Related application notes can be found here.

Features

  • High intensity with high resolution
  • Automated alignment of the multiple system configurations to optimize the measurement conditions every time
  • Automation of measurements and experiments:
    • » Allows very easy change between configurations
    • » Enables automatic measurements under recipe control
  • Works with leading edge analysis software (RADS, REFS..) for accurate and fast analysis (worldwide proven with over 100 installations)
  • No calibration samples required: X-ray metrology techniques are absolute
  • Non-destructive measurement techniques

Materials

The D1 Evolution can be used for virtually any thin film analysis. Some of the parameters which can be measured are:

  • Thickness
  • Composition
  • Relaxation
  • Strain
  • Area uniformity
  • Density
  • Roughness
  • Phase
  • Crystalline texture
  • Crystallinity
  • Residual stress
  • Pore size
  • Grain size

Techniques

Specification

Source

  • Standard 2.2kW sealed tube X-ray generator
  • Parabolic Multilayer Mirror
  • Choice of beam conditioning crystals for wide range of resolutions (5", 10", 12", 25")
  • Intelligent Alignment System, automatically configuring the tool with the best optics for the specified measurement

Sample Stage

  • Simple tilt / Z stage
  • Full Eulerian cradle with
    • » Highest resolution goniometer commercially available (0.16" resolution on Omega and 2Theta)
    • » Sub-micron resolution on all translation axes
    • » 150mm scanning on X and Y, with 200mm wafer capability
    • » 135o range on tilt (Chi) for pole figure and residual stress capability
    • » Full 360o range on Phi (rotation)
  • Vertical geometry to avoid gravity sag

Detection

  • High dynamic range scintillation detector (EDRc)
  • Choice of detector optics
    • » Dual channel triple axis analyzer crystal, with high intensity and high resolution channels for precise detector angle definition
    • » Soller slits for polycrystalline XRD work to allow a wide parallel beam into the detector - essential for glancing incidence XRD work
  • Motorized detector slits available
  • Intelligent Alignment System, automatically configuring the tool with the best optics for the specified measurement